展开剂
- 名Developing agent;developing solvent
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TLC条件为氯仿甲醇氨溶液(120∶20∶0.2)作展开剂;
The TLC conditions were as follows : The developing solvent was chloroform - methanol - ammonia solution ( 120 ∶ 20 ∶ 0.2 );
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以环己烷-乙酸乙酯(10:1)为展开剂,分离效果好,展开后Rf值适中,斑点清晰。
With cyclohexane-ethyl acetate ( 10:1 ) as the developing solvent , the separation effect is good , the Rf value after developing is moderate , and the spots are clear .
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方法选用不同的溶剂和展开剂,比较分离效果和Rf值。
Methods To choose the different dissolvent and developer , to compare the separating effect and Rf .
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以二-(2-乙基己基)磷酸酯(P(204))/四氢呋喃/硝酸/多聚乙醛为展开剂薄层色谱法分离铕、钆、铽、镝、钬、铒等元素
Separation of Rare Earth Elements ( Eu , Gd , Tb , Dy , Ho , Er ) by Thin-Layer Chromatography with Di - ( 2-ethylhexyl ) phosphate-Tetrahydro-furan-Nitric Acid-Paraldehyde System as Developer
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应用均匀实验设计及其数据处理,对脂肪酶催化维生素E与阿魏酸乙酯转酯生成维生素E阿魏酸酯的薄层色谱展开剂系统进行优化。
In this paper , the TLC developing solvent system for separating alpha-tocopheryl ferulate synthesized by the lipase-catalyzed reaction was optimized by the Uniform Experimential Design .
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桂枝:采用硅胶G板,以石油醚(60-90℃)&醋酸乙酯(17:3)为展开剂,显色剂为二硝基苯肼乙醇试液。
Cinnamon twig was identified with petroleum ether ( 60-90 ) - ethyl acetate ( 17:3 ) as developer and dinitrophenylhydrazine ethanol solution as coloration using silica gel G.
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选用硅酸G薄层板,展开剂为正己烷∶乙酸乙酯∶醋酸∶甲酸(6∶32∶1∶1);
Selection thin board of silica gel-G , it opened up is n-Hexane : Ethy 1 acetate : Acetic acid : formic acid ( 6 ∶ 32 ∶ 1 ∶ 1 );
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结果表明:两种萃取剂的萃取能力随展开剂的酸度不同而变化。N,N二苯基甘氨酸对5种金属离子的萃取能力强于N正丁基甘氨酸。
As shown by study the extracting powers of two extraction agents are changed with acidy of developer extracting power N , N-diphenyl glycine is stronger than N-n-butyl glycine for 5 metal ions .
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后者黄芩的鉴别:硅胶G薄层板,正丁醇-冰乙酸-水(7:1:2)为展开剂,1%三氯化铁乙醇溶液为显色剂;
The identification of Radix scutellariae was silica gel G plate , n-butanol-glacial acetic acid-water ( 7:1:2 ) as the development reagent , chloride ferric ( 1 % ) as color developing reagent .
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方法:薄层色谱法鉴别,采用以羧甲基纤维素钠为粘合剂的硅胶G薄层板,以醋酸丁酯甲酸水(7∶2.5∶2.5)上层溶液为展开剂;
Method : TLC method was used for identification with silica gel G plate and butyl acetate formic acid water ( 7 ∶ 2.5 ∶ 2.5 ) upper layer as a developing solvent .
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方法:薄层鉴别采用硅胶G薄层板,展开剂:正己烷-醋酸乙酯-冰醋酸(6:4:0.25),显色剂:10%硫酸乙醇溶液;
Methods : Qualitative analysis by TLC , a mixed solvent of n-hexane - ethyl acetate - acetic acid ( 6:4:0.25 ) was employed as the mobile phase , color developing agent was 10 % sulfuric acid and ethanol solution .
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同时通过反复试验,结合HPLC检测,确定了以展开剂氯仿:甲醇(90∶10)展开DON毒素的Rf值约为0.45。
Through ( repeated ) tests and HPLC examination , Rf value of DON for TLC was determined as 0.45 with chloroform-methanol ( 90 ∶ 10 , V / V ) as ( expanded ) material .
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薄层层析硅胶GF254为固定相,乙酸乙酯甲醇水(7-2-1,v/v/v)为展开剂,熊果苷和氢醌的Rf值分别为0.56和0.67。
The optimal conditions of TLC were as follows : silica gel GF254 as stationary phase , ethyl actate-methanol-water ( 7-2-1 , v / v / v ) as mobile phase .
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三萜醇乙酸酯和4-甲基甾醇乙酸酯是采用20%硝酸银-硅胶G薄板,并用二氯甲烷-石油醚(8:2v/v)作展开剂进行分离的。
The acetates of triterpene alcohols and 4-methylsterols are separated by TLC with 20 % silver nitrate impregnated silica gel G , using CH_2CL_2-petroleum ( 8:2v / v ) as developing reagents . The identification of major components is carried out by TLC , m.
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TLC法选用硅胶G板,展开剂:环已烷-乙酸乙酯(4∶1),测定波长:610nm,参比波长:420nm。
Silica gel plate was used in TLC with developer : cyclohexane ethyl acetate ( 4 ∶ 1 ), scan wavelength : 610 nm , reference wavelength : 420 nm .
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大黄:采用硅胶G板,以正己烷醋酸乙酯甲酸(30:10:0.5)为展开剂,于紫外灯下365nm检视。
Radix et Rhizoma Rhei was identified with n-hexane-ethyl acetate - formic acid ( 30 : 10 : 0.5 ) as developing agent in silica gel G plate .
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方法采用TLCS法,展开剂为正丁醇-冰乙酸-水(5∶1∶1),检测波长为345nm。
Methods n-butanol-acetic acid-water ( 5 ∶ 1 ∶ 1 ) was used as a developer , and detection wavelength was 345 nm .
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薄层色谱分析显示,葛根素精品在薄层板上呈蓝色荧光斑点,选用氯仿-甲醇(4:1)为展开剂,Rf为0.31;
The blue fluorescence spot on TLC was the sign of puerarin . Choose methanol - chloroform ( 4:1 ) as extending solvent , Its Rf was 0.31 . The data of nuclear magnetic resonance hydrogen spectrum accorded with characteristic of puerarin structure .
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方法:采用归胶G板和硅胶GF254板,用不同的展开剂分别对方中苦豆子、决明子和莱菔子进行薄层色谱(TLC)鉴别。
Methods : silica gel G and GF_ ( 254 ) thin layer plates were used and developed by different developing agents to identify the remedium cardinale-sophora seed , Cassia Seed and Radish Seed .
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用氯仿-甲醇-甲酸(20:1:0.2)为展开剂,在硅胶G-CMC-Na薄层板上分离齐墩果酸,10%硫酸乙醇溶液显色,用CAMAGⅡ型薄层扫描仪进行定量测定。
Oleanolic acid was developed with chloroform-methanol-formic acid ( 20:1:0.2 ), isolated on the silica gel G-CMC-Na thin-layer plate , colored with a 10 % ethanol sulfate solution , and quantified by the CAMAG ⅱ thin-layer scanner .
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用苯丙酮醋酸乙酯甲醇(7∶3∶3∶0.5)为展开剂,在硅胶GF254薄层板上分离槐果碱,然后定位、刮下、洗脱,采用紫外分光光度法进行含量测定。
Using benzene-acetone-ethyl acetate-methanol ( 7:3:3:0.5 ) as developing agent , sophocarpine was separated on silica gel GF254 TLC-plate , then located , scraped , eluted and determined by UV-spectrophotometry .
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方法:采用薄层色谱法常用的硅胶GF254薄层板,以醋酸乙酯-异丙醇-浓氨溶液(43∶35∶5)为展开剂,以自身对照法检查磷酸伯氨喹原料的有关物质。
Methods : The related substances were tested by TLC , the coating substances was GF254 , the mobile phase is a mixture of ethyl-isopropanol-concentrated ammonia solution ( 43 ∶ 35 ∶ 5 )( V / V ) .
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方法:采用日本岛津CS-930型双波长薄层扫描仪,含0.5%CMC-Na的硅胶G薄层板,展开剂:甲醇-氯仿(1:6),显色:碘蒸气。检测波长430nm,狭缝尺寸:2nm×2nm。
Method : The CS-930 dual-wavelength TLC scanner was selected , silic-gel thin-layer with 0.5 % CMC-Na solution , developing solvent : methanol-chloroform ( 1 : 6 ), coloration : iodine steam , the detection wavelength was 430 nm , slit size : 2 nm × 2 nm .
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方法:依据介电常数ε及文献常用的展开剂,采用U5(53)表以均匀设计布点。结果:以较快的速度获得补骨脂有效成分的分离条件。
Methods : Depending on dielectric constant ε of solvents and commonly used developers , the U 5 ( 5 3 ) tables were used to fulfil even design experimental scheme Results : The conditions of separation of effective components in psoralea fruit could be obtained with faster speed .
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罗沙替丁醋酸酯合成的薄层色谱展开剂的选择
Selecting Developing Agent in Synthesis Process of Roxatidine Acetate by TLC
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胱氨酸和酪氨酸纸层析分离的理想展开剂
Two Suitable Developing Solvents for Isolating Tyr and Cys by Paper Chromatography
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对展开剂作了探索,分离和测定结果令人满意。
The results of separation and determination were satisfactory .
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茚三酮直接加入展开剂显色的探索
A Method for Adding Ninhydrin Directly to Developing Agent
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一种新的展开剂用于氨基酸的薄层色谱分析
Application of a New Developer in Thin Layer Chromatographic Analysis of Amino Acids
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虫草菌丝体薄层色谱中两种展开剂的选择
Two kinds of developing solvent choices in Chinese caterpillar fungus mycelium thin layer chromatograph