一锅法
- 网络One-pot;one pot;one-pot synthesis;one-pot process
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在磷酸盐缓冲溶液-异辛烷混合溶剂中制备了固定化假单胞菌脂肪酶(PseudomonasCepaciaLipase,PSL)PSL/CS-MCM-48,并用于潜手性苯乙酮一锅法还原转酯化手性拆分反应。
The lipase ( Pseudomonas Cepacia Lipase , PSL ) was immobilized on the CS-MCM-48 in a mixed solvent of phosphate buffer solution and isooctane and used for one-pot reduction and transesterification synthesis of pure enantiomers from prochiral acetophenone .
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H2O2-HCl-HClO4三元体系一锅法水解壳聚糖制备盐酸氨基葡萄糖
Preparation of Glucosamine Hydrochloride by the H_2O_2-HCl-HClO_4 Ternary System One-pot Hydrolysis of Chitosan
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一锅法合成(E)-红霉素A肟的新工艺
One pot synthesis of ( E ) - erythromycin A oxime
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酶促酰化与Michael加成及串联一锅法合成含糖咪唑衍生物研究
Research on Enzymatic Acylation-Michael Addition and One-Pot Tandem Synthesis of Sugar-Containing Imidazole Derivatives
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此外,由XRD谱图还初步提出了一锅法乳液聚合的插层机理。
Further more , the mechanism of intercalation via one pot emulsion polymerization method was proposed by analysising XRD spectra systemically .
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水相中‘一锅法’Wittig反应的研究和手性P,O-配体的合成及其在不对称烯丙基烷基化反应中的应用
' One Pot ' Wittig Olefinations in Aqueous Media & Synthesis of Chiral P , O-Ligands and Their Application in Asymmetric Allylic Alkylation
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铜(II)酪氨酸乙酯络合物催化一锅法合成S(-)-1,1-′联萘-2,2′-二酚
One-Pot Synthesis of S - ( - ) - ( 1,1 ′ - Binaphthalene ) - 2,2 ′ - diol Catalyzed by Cu ( II ) - Tyrosine Ethyl Ester Complexes
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以氨基酸甲酯的盐酸盐为原料,用一锅法高产率地合成了一系列N-取代叔胺,其结构经1HNMR和MS表征。
A series of tertiary amines with high yield were synthesized by one step from methyl amino acid ester . The structures were characterized by ~ 1H NMR and MS.
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探讨了一锅法pH、温度敏感性壳聚糖基纳米颗粒的制备及其在氨基酸药物的释放上的研究。
The release rate of Vanillin can be adjusted by changing the temperature and pH. ( 3 ) The " one-pot " synthesis of pH - and temperature-sensitive chitosan nanoparticles and its application in amino acid delivery were investigated .
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用二(三氯甲基)碳酸酯(BTC)代替光气,“一锅法”合成了8种取代脲类除草剂,产物结构经元素分析、IR确证。
Eight substituted ureas herbicides were synthesized with bis ( trichloromethyl ) carbonate ( BTC ) . The production structures were identified by elemental analysis and IR .
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CLT酸的合成由专利的分批操作法改为工业化生产较为适宜的从原料到产品的一锅法合成。
The batch operation of CLT acid synthesis by Japanese patent has been changed to the once-through operation to fit for the industrialization production .
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考察了其作为催化剂在三组分苯甲醛、苯胺、环己酮一锅法Mannich反应中的应用,同时与常规的吡啶类碱性离子液体进行比较。
Novel ILs were applied to catalyze one-pot three component Mannich reaction of benzaldehyde , aniline and cyclohexanone in comparison with other conventional pyridine ILs .
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Yb(OTf)3催化苯乙酮、芳香醛和芳香胺的Mannich反应:三组分一锅法合成β-氨基酮衍生物
Yb ( OTf ) _3 Catalyzed Mannich Reaction of Acetophenone with Aromatic Aldehydes and Aromatic Amines : Three Component One-pot Synthesis of β - Amino Ketone Derivatives
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以硝化纤维素为原料,经一锅法醚化和胺化2步反应合成了仲胺型硝化纤维素(ACN)。
The cellulose nitrate containing secondary amine group ( ACN ) was prepared by one-pot method in two steps : etherification and amination .
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一锅法合成甲基丙烯酰基封端的PLA-PEG-PLA大分子单体
One-Pot Synthesis of Macromer of PLA-PEG-PLA Terminated with Methacryloyl Moiety
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CS-MCM-48复合载体固定化脂肪酶催化苯乙酮一锅法还原转酯化拆分反应
One-pot Reduction and Transesterification Resolution of Acetophenone Catalyzed by Lipase Immobilized on MCM-48 Coated Chitosan
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报道了碘催化下芳香酮、芳香醛和芳香胺的Mannich反应,三组分一锅法合成了一系列的β-胺基酮衍生物,该方法操作简单、条件温和、产率较高。
The three component " one-pot " Mannich reaction of aromatic ketones with aromatic aldehydes and aromatic amines catalyzed by iodine afforded the corresponding β - amino ketone derivatives in high yields under mild conditions .
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化合物的结构通过1H-NMR、13C-NMR及MS进行了表征确认。该路线中磺化和硝化两步反应采用了一锅法,减少了试剂用量,缩短了反应时间,并减少了中间产物在处理过程中的损失。
The target products were characterized by ' H-NMR , 13C-NMR and MS. In addition , a one-pot reaction was used in the two steps of sulfonation and nitration , which reduced the amount of reagent , reaction time and the loss of the intermediate product .
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以丙二腈为原料,用一锅法合成了呋咱类含能化合物3-氨基-4-氨基肟基呋咱(AAOF),收率72.4%。
A new energetic furazano compound , 3-amino-4-aminoximidofurazan ( AAOF ), was synthesized in yield of 72.4 % using dicyanopropane as initial material by one-pot method .
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采用一锅法自动化合成18F-FAC,操作简便,能满足科研和临床正电子发射断层显像的需要。
18F-FAC injection is easy to be obtained and can be used for clinical and scientific study with positron emission tomography ( PET ) imaging .
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以丙二腈为原料经四步连续反应一锅法合成出了新型含能材料化合物3氨基4氨基肟基呋咱(AAOF),得率达72.4%。
A new energetic material compound 3-amino-4-aminoximinofurazan ( AAOF ) with yield of 72.4 % was synthesized by using dicyanopropane as initial material through 4-step continuous reaction by one-pot method .
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采用自制的X-903型高压苎麻脱胶机,进行一锅法连续化苎麻脱胶,其精干麻质量达到或超过传统的脱胶工艺。
Ramie continuous degumming in one bath was carried out on a high pressure ramie degumming machine X-903 , and good degumming effects were obtained . The quatity of degummed ramie attained or exceeded that with traditional process .
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一锅法合成月桂酸二乙醇酰胺的研究
Study on Synthesis of Lauric Acid Diethanolamide with One Pot Method
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微波辐射下一锅法合成3,4-乙撑二氧噻吩类化合物
One-pot synthesis of 3,4-dioxane ethylene thiophene compounds via microwave irradiation route
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一锅法的碳-碳双键形成反应。
" One - pot " carbon - carbon double bond formation .
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二(三氯甲基)碳酸酯一锅法合成取代脲类除草剂
One-pot Preparation of Substituted Ureas Herbicides with Bis ( trichloromethyl ) Carbonate
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酚羟基从乙酰基保护到苄基保护的一锅法转换
A One-Pot Conversion of Acetyl Protection to Benzyl Protection of Phenol Hydroxyl
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一锅法合成手性双取代不对称脲
One-pot Synthesis of Chiral N , N ' - Unsymmetrically Disubstituted Urea
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直馏柴油应用离子液体一锅法脱硫
" One pot " desulfurization of straight-run diesel oil with ionic liquid
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无溶剂一锅法合成1,4-二氢吡啶
One - pot Synthesis of Dihydropyridines under Solvent-free Condition