菲醌

菲醌法燃气脱硫的研究

Study of the desulphurization of gas with phenanthraquinone

菲醌的合成方法研究

On Synthesis Method of Phenanthraquinone

以菲醌为原料合成了标题化合物，通过IR和1HNMR对其结构进行了表征。

The title compound was synthesized with phenanthrenequinone as starting material and was characterized by IR and 1H NMR spectra .

由菲醌一步合成9－羟基－9－芴羧酸（HFC）。

Hydroxyl - 9 - fluorene carboxylic acid ( HFC ) is synthesized from phenanthrene dione .

菲醌单缩氨硫脲作为分析试剂的究研Ⅰ.试剂的合成与铜的光度法测定

Research of PTS as an Analytical Reagent

菲醌的合成及利用

Synthesis of Phenanthraquinone and its Use

通过电化学实验的测试，可以观察到两对明显的伏安波。这两对峰被归属为来自碳颗粒表面的外围菲醌官能团。

In electrochemical measurements , two pairs of well-defined voltammetric waves were observed , which might be ascribed to the peripheral functional moieties that were analogous to phenanthrenequinone derivatives .

研究了在溶剂LR中用高锰酸钾氧化菲制取菲醌，并探讨了合成菲醌的主要影响因素，找出了较佳工艺条件。

Oxidation of phenanthrene for the preparation of phenanthrenequinone was studied by potassium permanganate in LR in the paper .

高效液相催化氧化菲制取菲醌

Catalytic Oxidation of Crude Phenanthrene to Phenanthrenequinone in Liquid Phase

脉冲辐解测定邻菲咯啉醌的单电子还原电位

One electron redox of ortho-phenanthroline quinone studied by pulse radiolysis

本文以三氧化铬&乙酸为氧化剂，由工业菲制备菲醌。

Phenanthrenequinone was made from industrial phenanthrene with chromium trioxide-acetic acid as oxidant .

1,10-菲咯啉-5,6-醌水溶液的γ辐解

Gamma radiolysis of aqueous solutions of 1,10-phenanthroline-5,6-quinone

由工业菲制备菲醌

Preparation of Phenanthrenequinone from industrial phenanthrene

以纯度为84.21%的工业菲为原料，冰醋酸作溶剂，卤素化合物作为氧化剂氧化菲合成菲醌的氧化体系，菲醌最高收率可达63.23%，并确定了影响此反应的主要因素和最佳反应条件。

In the paper , phenanthrenequinone was prepared by oxidation of phenanthrene (( 84.21 % )) with halogen compound in the presence of glacial acetic acid . The yield of phenanthrenequinone can reach 63.23 % . Chief influential factors and optimum processing condition of this reaction were discussed .

实验结果表明：重结晶法提纯工业菲效果较好，能使菲的纯度由60.34%提高到84.21%，为后续菲氧化合成菲醌提供了原料。

The results indicate that the recrystallization has a good effect , the purity increase from 60.34 % to 84.21 % , and it can provides the raw materials for the synthesis of phenanthrenequinone .