固相反应法

结果表明：固相反应法可制得均一钙钛矿结构的LSC氧化物，柠檬酸法除制得LSC氧化物外，还有LaSrCoO4相的生成。

The experimental results show that the single perovskite phase of LSC can be synthesized by solid state reaction method , but LaSrCoO_4 phase appears in LSC powder synthesized by citric acid-nitrate low temperature self-propagating combustion method .

SrZrO3：Eu~（3+）：分别采用高温固相反应法和溶胶-凝胶法合成了SrZrO3：Eu~（3+）荧光材料。

SrZrO_3 : Eu ~ ( 3 + ) phosphor powders were synthesized by solid state reaction method and sol-gel method .

低温固相反应法合成水分散性CdS纳米晶

Solid State Synthesis of Water-Dispersive CdS Nanoparticles at Room Temperature

采用室温固相反应法合成了甘氨酸锑和苯丙氨酸锑双核配合物，用元素分析、远红外光谱、热重差热分析及X射线粉末衍射进行了表征。

The compositions and structures of the obtained complexes had been characterized by elemental analyses , far-infrared spectra , TG-DTA and X-ray powder diffraction .

固相反应法合成的巯基乙酸钠修饰ZnS的光催化性能

Photocatalytic Performance of Sodium Thioglycolate Modified ZnS Synthesized by Room Temperature Solid Phase Method

研究了在用不同方法（SHS方法和传统固相反应法）制备NiZn软磁铁氧体粉体的过程中，Zn挥发量的变化。

Zinc volatilization in the process of preparing Ni Zn ferrite powders by SHS and conventional solid phase method was investigated .

采用固相反应法合成了Cu掺杂的高温氧渗透膜材料，并用于甲烷部分氧化制合成气反应过程。

Cu doped oxygen permeating membrane materials were synthesized by solid state method and it was used in the process of the partial oxidation of methane to syngas .

新的固相反应法合成钼青铜化合物NaxMo6O（17）的研究

A New Synthetic Method for Molybdenum Bronze Na_xMo_6O_ ( 17 ) by Solid Phase Reaction

Li4Ti5O（12）电极材料的二步煅烧固相反应法合成及炭包覆改性研究

Study on Solid State Reaction Synthesis by Two-step Calcination and Carbon-coated Modification of Li_4Ti_5O_ ( 12 ) Electrode Material

尖晶石LiMn2O4前驱体的低热固相反应法合成机理及其结构与热分解过程研究

Structure , Preparation Mechanism and Thermo decomposition Process of LiMn_2O_4 Precursor Prepared by Low heating Solid state Reaction

应用固相反应法于惰性气氛下合成掺Zr的LiFePO4正极材料。

Stoichiometric Zr-doped lithium iron phosphate ( LiFePO_ ( 4 )) cathode material was synthesized by a solid-state reaction in an inert atmosphere .

采用固相反应法用不同的烧结速率在1850℃烧结合成过烧钇铝石榴石（YAG）陶瓷，YAG陶瓷晶界形貌随烧结速率的变化而不同。

Oversintered YAG ceramics were synthesized at different sintering rates by solid-state reaction method at1850 ℃, and the morphology of YAG ceramics grain boundary changed with different heating rates .

该方法克服了固相反应法混合不均匀，反应不完整，样品重现性差和Tc较低的缺点；

It has overcome the shortcomings of inhomogeneous composition , incomplete reaction , low reappearance rate and Tc , which has be caused by the solid reaction method .

用微波法，固相反应法，超声法等方法制备Bi2S3纳米晶。

Many other methods such as microwave irradiation , solid state reaction , sonochemical method were also used to prepare Bi_2S_3 nanocrystals in this study .

采用固相反应法合成了SrCoO2.5+δ样品，用XRD表征了在空气和纯氧气氛下自然降温以及淬火后SrCoO2.5+δ的结构；

The SrCoO_ ( 2.5 + δ) was synthesized by solid state reaction , and the structures of different samples cooling under air and pure oxygen atmosphere were characterized by XRD .

固相反应法、柠檬酸盐法制备（NaBi）（0.5）TiO3陶瓷及性能表征

Characterization of ( NaBi ) _ ( 0.5 ) TiO_3 Ceramic Fabricated by Solid Reaction and Citrate Method

结合部分草酸铅固相反应法的优点对共沉淀法进行改进，发展了一种合成锆钛酸铅（PZT）粉体新工艺。

A new coprecipitation route has been developed for the synthesis of lead zirconate titanate by combining the advantages of partial lead oxalate solid-reaction method and coprecipitation method .

以Zn（NO3）2和NaOH为原料，用液相反应法及室温固相反应法首先合成出Zn（OH）2，再将Zn（OH）2热分解得到纳米ZnO。

Zn ( OH ) 2 was synthesized by both liquid reaction and solid reaction with Zn ( NO 3 ) 2 and NaOH as raw materials . Nanometer ZnO was obtained by hot decomposition .

自主开发了制备高惰性C18硅胶填料的新型气固相反应法。

A novel gas-solid reaction method for the preparation of highly deactivated octadecyl ( C18 ) bonded silica packing was developed independently .

以Li2CO3和NH4VO3为原料，采用非熔融态的固相反应法合成了锂离子电池正极材料锂钒氧化物。

Lithium vanadium oxide , as cathode material for Li-ion battery , was synthesized by non-molten solid-state reaction with Li_2CO_3 and NH_4VO_3 as raw materials .

首次研究了以无定形TiO2为原料，通过固相反应法和溶胶-凝胶法二种工艺合成Li4Ti5O（12），实现了原料和工艺低成本化。

Synthesizing technologies of Li_4Ti_5O_12 with amorphous TiO_2 as raw materials were firstly exploited by conventional solid phase reaction and sol-gel method , and the cost of materials and technologies are lower than other .

按照化学摩尔配比计算原料、采用固相反应法合成了Na0.7CoO2样品，XRD测量结果表明合成的Na0.7CoO2是单相多晶。

The samples of Na_ ( 0.7 ) CoO_2 polycrystals have been synthesized by solid-state reaction according to corresponding components chemical molar ratio . The result of XRD measurements has demonstrated shown that the Na_ ( 0.7 ) CoO_2 samples are of the single-phase polycrystals .

以SnCl4·5H2O，Zn（NO3）2·6H2O和NaOH为原料，用低温固相反应法合成尖晶石型复合氧化物Zn2SnO4纳米晶体。

Single phase spinel type composite oxide Zn_2SnO_4 nanocrystals were prepared by solid state reaction at low temperature using SnCl_4 · 5H_2O , Zn ( NO_3 ) _2 · 6H_2O and NaOH as raw materials .

以MgAC2为掺杂源，采用固相反应法在惰性气氛下合成了掺Mg的LiFePO4正极材料，考察了Mg2+对于目标化合物物理及电化学性能的影响。

Stoichiometric Mg-doped lithium iron phosphate ( LiFePO_4 ) cathode material was synthesized by a solid-state reaction in an inert atmosphere which used MgAC_2 as dopant . The effects of Mg ~ ( 2 + ) doping on the physical and electrochemical properties of as-synthesized cathode materials were investigated .

采用固相反应法和柠檬酸-硝酸盐溶胶-凝胶低温自蔓延燃烧法（简称柠檬酸法）合成了La0.5Sr0.5CoO2.91（LSC）复合氧化物。

Compositely doped oxide La_ ( 0.5 ) Sr_ ( 0.5 ) CoO_ ( 2.91 )( LSC ) was synthesized using solid state reaction and citric acid-nitrate low temperature self-propagating combustion methods .

分别采用固相反应法和溶胶凝胶法制备SnO2基体材料，以Sb2O3为降阻剂，在不同温度下烧结，制得SnO2气体传感器。

SnO_2 gas sensor is prepared at different sinter temperature using SnO_2 material produced by solid reactivity method and sol-gel method respectively , with Sb_2O_3 as drop resistance solution .

XRD显示在1350℃煅烧就能得到单相的CaAl2O4基质，相对于高温固相反应法烧结温度降低了150℃；

The XRD patterns show that the product prepared at 1 350 ℃ is single phase CaAl_2O_4 host , which is 150 ℃ lower than that of high temperature solid state reaction .

针对skutterudite材料制备工艺中熔融法和固相反应法合成周期长、工序多的不足，尝试将机械合金化法应用于skutterudite材料制备中。

Considering that melting and solid state reaction methods are complex and time - consuming in preparing skutterudite materials , mechanical alloying is selected to be studed .

我们用固相反应法成功合成了MgxB2（0.5x1.3）系列样品，并对其结构，临界电流密度（Jc）和不可逆场（Hirr）进行了研究。

Bulk samples of Mg_x B_2 ( 0.5 x 1.3 ) starting composition were prepared using a solid-state reaction route . Their structure , critical current density ( J_c ) and irreversibility field ( H_irr ) were investigated .

用固相反应法合成了碘化砷、氯化锑与硫脲（Tu）和半胱氨酸（Cys）的配合物，用元素分析、IR及X射线粉末衍射进行了表征。

The cysteine ( Cys ) and thiourea ( Tu ) complexes with antimony and arsenic trihalide have been synthesized by solid phase reaction . The compositions and structures of the complexes have been characterized by elemental analysis , infrared spectra and X ray powder diffraction .