中乌头碱

方法中所用试剂成本低、毒性小，适用于乌头碱、中乌头碱、次乌头碱的提取分离以及对照品的制备。

This method was at low cost , harmless and suitable for extracting , separating and preparing mesaconitine , aconitine and hypaconitine .

HPLC测定小金胶囊中乌头碱的含量

HPLC assaying of aconitine in Xiaojin capsules

目的：建立HPLC法测定三乌胶中乌头碱限量的检查方法。

Objective : A HPLC method was established for the detection of aconitine in sanwujiao .

盐酸美金刚胶囊人体药代动力学研究HPLC测定小金胶囊中乌头碱的含量

Pharmacokinetics of memantine hydrochloride capsule in Chinese healthy volunteers HPLC assaying of aconitine in Xiaojin capsules

本文探讨了测定小活络丸中乌头碱溶出度的方法。用浆法，以pH3的70%乙醇液为介质，转速为100r。

The determination method , using paddle method , for dissolution rate of aconitine from Xiaohuoluo Pills was studied ( medium : 70 % alcohol , pH3 , rotation speed : 100 . r. p. m ) .

结论该方法灵敏、快速、准确，适用于生药、饮片、药酒中乌头碱的检测。

Conclusion This method was sensitive , fast and accurate .

复方酒剂中乌头碱含量的测定及其中毒剂量的研究

Determination of Aconitine in Medicinal Wine and Its Dosage of Aconitine Poisoning

生物检材中乌头碱的GC/MS分析

Detection of aconitine in biological samples by GC / MS

兔血液中乌头碱代谢产物的研究

Study on the Metabolites of Aconitine in Rabbit Blood

关于《中国药典》中乌头碱限量检查法改进

Improvement of Limit Test of Aconitine in Chinese Pharmacopeia

复方中药四逆汤中乌头碱类二萜生物碱的电喷雾串联质谱研究

Studies on the Aconitum Alkaloids in the Sini Concoction by Electrospray Ionization Mass Spectrometry

目的：建立蒙药巴特日七味丸中乌头碱的含量测定方法。

Objective : to establish a method for assay of aconitine in Garidi-qiwei pill .

不同时间内家兔尿液中乌头碱代谢产物的研究

Study on metabolites of aconitine in rabbit urine collected at different times after administration

目的建立GC/MS-SIM检测生物检材中乌头碱的定性方法。

Objective To establish a method used for qualitative determination of aconitine in biological samples by GC / MS.

目的建立血液中乌头碱、次乌头碱、新乌头碱的LC/MS/MS分析方法。

Objective To establish a method used for determination of Aconitine and Hypaconitine and Mesaconitine in blood by LC / MS / MS.

为了解其中原因，本实验采用酸性染料比色法，测定了附子药液及经不同量的活性碳吸附后附子药液中乌头碱类生物碱的含量。

Acid dye colorimetry was used for quantitative determination of aconitine_type in the extraction of Radix Aconiti Praeparata which was adsorbed by different concentration of activated charcoal .

目的比较纤维素酶、半仿生、乙醇回流提取方法对川乌中乌头碱、乌头总碱的影响，筛选最佳方法。

Objective To compare the extraction methods of cellulose enzyme , semi-bionic and alcohol reflux for the impact of aconitine and aconitum alkaloids yields , and to optimize the extraction method .

单煎与混煎组方中乌头碱的含量均随着大黄剂量的增加而减少，两者均呈线性相关。

The content of aconitine in the single decoction recipe and combined decoction recipe would decrease with a decrease of rhubarb dose and would be presented by liner correlation in two recipes .

结论LC/MS/MS法灵敏可靠，样品处理快速简便，适用于血液中乌头碱、次乌头碱、新乌头碱的检测。

Conclusion The method of LC / MS / MS is sensitive and reliable , and the sample handling is quick and simple , which was suitable for determination of the Aconitine and Hypaconitine and Mesaconitine in blood sample .

此法亦应用于14个不同的乌头属药材及10个不同的中成药样品中的乌头碱含量检测。

The method was applied to the analysis of 14 samples of various species of Aconitum plants and 10 different proprietary medicine samples .

比较在不同pH的缓冲液溶剂中，新乌头碱体外渗透速率的差异。

To compare the percutaneous speed ( J ) of MA with different pH buffer solution .

在最佳分离条件下对中草药中乌头碱及次乌头碱含量进行了测定。

The content of the aconitine and hypaconitine in Aconitum medicinal herbs were determined under the optimum separation conditions .

结论：本方法检测乌头类生物碱的含量，效果颇佳，色谱图中3种乌头碱的特征峰明显，与其他峰的分离也较好，完全能够满足这3种乌头类生物碱质量检测标准的要求。

In the chromatograms of the three aconitine-type alkaloids , there are clear characteristic peaks , distinguishing well from other peaks , which meet well the requirement of the criteria on detecting the quality of the three aconitine-type alkaloids .

体内法表明伤痛外搽酊低、高剂量组家兔血液中均未检出乌头碱，低剂量组家兔血液中未检出士的宁，高剂量组家兔血液中士的宁含量为32.44ng/ml。

In vivo test indicated that there are not aconitine in the rabbits bloods of low and high dosage . The low dosage are not strychnine . The strychnine in rabbits bloods of the high dosage was penetrated 32.44ng/ml .

小活络丸中痕量毒性成分乌头碱的快速限量检测

Fast limit test of trace aconitine in Xiaohuoluo Pills

对结果进行分析显示四种样品溶液中均未检出乌头碱，附子单煎与附子配伍甘草未检出新乌头碱。

The results showed that four decotion of SND compatibility had not detected aconitine , Fuzi single and Fuzi combined with Gancao had not detected new aconitine .

肾气丸阴中求阳配伍对方中乌头碱和次乌头碱含量的影响

Influence of Compatibility of Shenqi-Pill " Reinforcing Yang from Yin " on the Content of Aconitine and Hypaconitine in the Decoction