3-Nitrobenzaldehyde
3-Nitrobenzaldehyde-
Study of the solid state condensation reaction between 3-nitrobenzaldehyde and thiobarbituric acid
3-硝基苯甲醛与硫代巴比妥酸固相反应的研究
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The solid state reaction of 3-nitrobenzaldehyde and 2-thiobarbituric acid was carried out .
研究了3-硝基苯甲醛与硫代巴比妥酸固相反应，选择了反应的最佳条件。
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Under microwave irradiation without solvent , the condensation of 3-nitrobenzaldehyde and acetoacetic ester took place in much shorter time than conventional ways . The yield approach or exceed those of conventional ways .
微波无溶剂条件下，3-硝基苯甲醛和乙酰乙酸酯进行缩合反应，反应时间较传统方法大大缩短，而且收率达到或超过了传统方法。