磺酰氯

所得中间体2-（甲硫基）乙基特戊酸酯低温下经磺酰氯氧化，与中间体3-氨基-4-氯苯甲酸甲酯反应，所得产物经重排、水解和酰化反应得到目标化合物，总产率25.8%。

2 - ( Methylthio ) ethyl pivalate was oxidized by sulfuryl chloride , and then reacted with methyl 3-amino-4-chlorobenzoate followed by rearrangement , hydrolysis and acylation to give the title compound in overall yield of 25.8 % .

以S-烃基异硫脲盐、硫氰酸酯、硫醚为底物，在盐酸介质中，温和条件下，通过氧化法高产率地合成了烃基磺酰氯；

Hydrocarbyl sulfuryl chloride was prepared by the oxidation of S - hydrocarbyl isothiouronium salts , thiocyanic esters and sulfuric ether in the medium of hydrochloric acid under mild conditions with high yields .

研究通过丹磺酰氯柱前衍生，用HPLC对纳豆发酵过程中的生物胺进行检测。

Biogenic amines during the fermentation of natto was detected by HPLC , using precolumn derivatization with DNS-Cl.

氯化介质中PbS固体表面的氯络合-溶解行为第三组仅加完全培养基。正十六烷基磺酰氯的合成

Complexation and Dissolution at the Surface of Solid PbS in Chloride Medium

二乙醇胺和对甲苯磺酰氯在三乙胺存在下，反应生成N，0，O′－三（对甲苯磺酰基）双（2－羟乙基）胺，产率93%。

In the presence of triethylamine , N , O , O ' - tris ( p-toluenesulfonyl ) his ( 2-hydroxyethyl ) amine was prepared in 93 % yield by tosylation of diethanolamine with p-toluenesulfonyl chloride .

由氨基酸组成求得最小分子量约16500。（4）用二硝基氟苯，二甲基氨基萘磺酰氯及氨肽酶M测定抑制剂A、B的N末端，都证实是天冬氨酸。

The minimum molecular weights as estimated from the amino acid compositions were about 16,500 . For both inhibitors A and B the N-terminal amino acid was aspartic acid , as determined by the FDNB and DNS-Gl methods and further confirmed by enzymic hydrolysis with aminopeptidase M.

化合物2再在三乙胺作用下与2mol的甲烷磺酰氯反应制成甲磺酸酯（3）；

The compound 2 then reacted with 2 equiv. of methylsulfonyl chloride and 3 equiv.

利用静态荧光技术系统研究了5-二甲氨基萘磺酰氯（DNS-Cl）在丙酮中簇集行为。

The aggregation of dansyl chloride ( DNS-Cl ) in acetone has been studied in detail by steady-state fluorecence techniques .

通过苯磺酰氯与氨基之间的反应制备了含不同比例氨基和DNQ的光温双敏感微凝胶纳米粒子。

Via the reaction between sulphonyl chloride and amino group , photo - / thermo-responsive microgels were prepared with different ratios of DNQ to amino groups .

用氧化还原电位滴定法测定磺酰氯的含量

Determination of Sulphonyl Chlorides by Potentiometric Titration Based on Oxidizing-reduction Principle

以氯苯为原料，合成了对氯苯磺酰氯。

Chlorobenzene sulfonyl chloride was synthesized with chlorobenzene as raw material .

荧光素和苯磺酰氯间反应机理研究

Study on the Reaction Mechanism Between Fluorescein and Phenylsulfonic Acid Chloride

对甲基苯磺酰氯生产工艺的改进

Improvement on p - methyl benzene sulfonic chloride production process

测定2-重氮-1萘醌-5-磺酰氯的含量

The Content of 2 diazo 1 Naphthoquinones 5 Sulfonyl Chloride is Determined

以5-二甲氨基萘磺酰氯为荧光探针的功能膜制备

Preparation of Functional Film on Dansyl Chloride as Fluorescence Probe

酞菁铜磺酰氯接枝聚苯胺的合成与表征

Synthesis of Polyaniline Grafted by Cu Chloric Sulfonic Acid Phthalocyanine

四个香豆素磺酰氯衍生物的合成及其荧光性能的研究

Synthesis and Study of Fluorogenic Property Four Kinds of Coumarin Sulphonyl Chloride Derivatives

高纯度3-硝基-4-氯苯磺酰氯的制备

Synthesis of 4-chloro-3-nitrobenzene sulfonyl chloride with higher purity

烷基磺酰氯在皮革化工中的应用

Application of Alkanesulfonyl Choride in Leather Chemical Industry

提高甲烷磺酰氯收率的方法

Study on Increasing the Yield of Methanesulfonyl Chloride

甲烷磺酰氯的合成研究

Study on the Synthesis of Methane Sulfonyl Chloride

红外光谱法研究聚苯乙烯磺酰氯树脂功能基团的均一性

Study on the Function Group Uniformity of Polystyrol Sulfonyl Chloride Resins by Infrared Spectra

工业苯磺酰氯测定方法的选择

Selection of Industrial Benzene Sulfonyl Chloride Analytic Method

氯代烷基磺酰氯衍生物的合成及其应用

Synthesis and Application of Chlorinated Alkyl Sulfonamide Derivates

2,1,5-磺酰氯合成的研究

Study on Synthesis of 2,1,5-Sulfonyl Chloride

对甲苯磺酰氯的合成研究

Study Synthesis of p-Toluenesulfonyl Chloride

碳酸氢铵生产母液中烷基磺酰氯测定&混合指示剂两相滴定法

Determination of alkyl sulfonyl chloride in the ammonium acid carbonate mother solution by mixed indicate two phases titration

以4-甲苯磺酰氯活化的棉纤维为载体，对固定化菊粉酶的条件进行探讨。

Inulinase from Aspergillus ficuum SK004 was immobilized on cotton cloth activated with p-toluenesulfonyl chloride ( tosyl chloride ) .

同时，还改进了对甲苯磺酰氯和对甲苯磺酰甘氨酸的合成方法。

The improved methods for the syntheses of tolylsulfonyl chloride and Np-tolysulfonyl amino acids have been described in this work .

本文以硫化钠和对甲苯磺酰氯为原料，对对甲苯硫代磺酸钠的合成工艺进行了改进。

P-Toluene thio sulfonic acid sodium salt has been synthesized with sodium sulfide and p-toluenesulfonyl chloride as the raw materials .