邻苯二甲酰亚胺
- 名phthalimide
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报道了通过盖布瑞尔合成法制备N(2羟乙基)邻苯二甲酰亚胺。
The synthesis of N - ( 2-hydroxyethyl ) phthalimide via Gabriel synthesis method was reported .
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邻苯二甲酰亚胺和靛红的存在形态及SERS研究
The existing form and SERS study of phthalimide and isatin
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KF/Al2O3催化邻苯二甲酰亚胺的N-苄基化
N-Benzylation of phthalimide under the action of Al_2O_3 supported KF reagent
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N苯基邻苯二甲酰亚胺和N对甲苯基邻苯二甲酰亚胺的晶体和分子结构
Crystal and Molecular Structures of N - ( Phenyl ) phthalic Imidine and N - ( p-Methylphenyl ) phthalic Imidine
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然后在70°C条件下,以邻苯二甲酰亚胺钾作为亲核试剂,与2-氯-5-氯甲基吡啶发生缩合反应,制备了N-(6-氯-3-吡啶甲基)邻苯二甲酰亚胺。
Afterwards , N - ( 6-chloro-3-pyridinemethyl ) phthalimide is prepared by using potassium phthalimide , as nucleophilic reagent , condensation reacting with 2-chloro-5-methylpyridine at a temperature of 70 ° C.
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以聚苯乙烯-吡淀树脂为催化剂,催化合成了两种N-取代邻苯二甲酰亚胺,催化效果良好,催化剂可重复使用。
This paper has synthesis two kinds of N-Substituted phthalimides under the catalysis of polystyrene - pyridine resin . The catalysis is obvious and the catalyst can be reused .
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以DMF为溶剂,邻苯二甲酰亚胺钾盐与氯乙醇在90℃下反应12h,N(2羟乙基)邻苯二甲酰亚胺的收率为86%。
Potassium phthalimide reacted with 2-chloroethanol under 90 ? ℃ or 12 ? h in DMF solvent , and the isolation yield was about 86 % .
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CEL溶液中二磺酸基二邻苯二甲酰亚胺甲基酞菁锌的电子吸收和荧光光谱
Study on the Aggregation State of Sulfonated Phthalimidomethyl Zinc Phthalocyanine in CEL Solution
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缩合产物再经过硝化,合成N-(5-硝基-6-氯-3-吡啶甲基)邻苯二甲酰亚胺,其熔点为143.1~143.8°C,收率为90.5%。
Then , N - ( 5-nitro-6-chloro-3-pyridinemethyl ) phthalimide is obtained after the nitrating reaction of N - ( 6-chloro-3-pyridine methyl ) phthalimide . The yield of the obtained product is 90.5 % , and its melting point is 143.1 ~ 143.8 (° C ) .
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报道了以N–羟基邻苯二甲酰亚胺(NHPI)/过渡金属为催化剂,乙酸为反应介质,氧气为氧化剂,催化甲苯氧化。
Oxidation of toluene catalyzed by N – hydroxyphthalimide ( NHPI ) / transitions metals with molecular oxygen in the acetic acid reaction medium was reported .
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其中N4溴丁基邻苯二甲酰亚胺(1)改用相转移催化法合成,收率由文献的65%提高到88%。
N ( 4 bromobutyl ) phthalimide was prepared by a phase transfer catalyst in 88 % yield .
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试验证明以N-氯代邻苯二甲酰亚胺(NCP)为开环试剂,并用4A型分子筛为酸清除剂,在甲苯中回流反应2h可顺利开环。
The penicillin sulfoxide ester reacted with N-chlorophthalimide ( NCP ) in toluene for 2 h under reflux to break the ring , and 4A molecular sieve was used as acid scavenger in the process .
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邻苯二甲酰亚胺酰胺类手性分子钳的合成及其光学性能
Synthesis of Phthalimido Amide Chiral Molecular Tweezers and Their Optical Properties
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N-(N-叔丁基芳酰氨基)邻苯二甲酰亚胺的合成及其杀虫活性
Synthesis and Insecticidal Activity of N - ( N-t-Butylarylacylamino ) Phthalimide
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N-(2-甲胺基乙基)邻苯二甲酰亚胺盐酸盐的合成
Synthesis of N - ( 2-Methylaminoethyl ) phthalimide Hydrochloride
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四-邻苯二甲酰亚胺甲基酞菁锌的两种合成方法比较
Compare Two Methods for Synthesis of Phthalimidomethyl Phthalocyanine Zinc
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邻苯二甲酰亚胺衍生物的紫外光谱研究
Study on UV Spectra of Derivatives of Phthalimide
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N-(6-氯-1-氧-3-吡啶甲基)邻苯二甲酰亚胺的合成
Synthesis of N - ( 6-Chloro-1-oxy-3-pyridinemethyl ) phthalimide
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双(羧基邻苯二甲酰亚胺)的合成及其固化环氧树脂的研究
A Study on Synthesis Bis ( carboxyphthalimide ) sand Its Epoxy Resin Cured by It
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溶剂可回收循环使用。氨水循环法制备邻苯二甲酰亚胺
The solvent can be retrieved and circulated use . Preparation of Phthalimide by Recycling Ammonia
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氨水循环法制备邻苯二甲酰亚胺
Preparation of Phthalimide by Recycling Ammonia
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邻苯二甲酰亚胺的制备及应用前景
Preparation and Application of phthalimide
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聚苯乙烯固载聚乙二醇在邻苯二甲酰亚胺的N-烃基化反应中的相转移催化作用
A Study on the Phase Transfer Catalytic Effects of Polystyrene Supported Polyethylene Glycols on the N-alkylation of Phthalimide
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几种酰亚胺和酰胺的N-烷基化反应&邻苯二甲酰亚胺、琥珀酰亚胺和乙酰苯胺在相转移条件下N-烷基化反应的研究
N-Alkylation of Several Imides and Amides & A Study of the N-Alkylation of Phthalimide , Succinimide and Acetanilide Under Phase-Transfer Conditions
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该法先在室温条件下以邻苯二甲酰亚胺与氢氧化钾反应合成了邻苯二甲酰亚胺钾。
The method is presented as follows : firstly , potassium phthalimide is synthesized by phthalimide reacting with potassium hydroxide at the room temperature .
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着重介绍邻苯二甲酰亚胺的性质和各种制备方法及在农药、医药、染料、橡胶等行业中的应用前景,并对其市场作了分析。
This paper discusses the property , preparation and application of phthalimide in pesticide , medicine , dyes and rubber industry , and also presents opinions on its market prospects .
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其选择性大于70‰。邻苯二甲腈和邻苯二甲酰亚胺的重量收率大于90‰,添加P2O5的P型催化剂表现出了好的活性和选择性。
The selectivity is > 70 % phthalonitrile and phthalimide with > 90 % weight yield The P-catalyst containing P_2 O_5 shows good activity and selectivity .
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针对邻二甲苯氨氧化容易生成邻苯二甲酰亚胺的特点,筛选了选择性较高的ODT-88催化剂。
The selectivity of phthalonitrile is a key problem for the ammoxidation of o-xylene . Based on appraising tests , a catalyst ODT-88 of higher selectivity has been found .
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首先,从邻苯二甲酸酐(Ⅱ)和(R)-(-)-苯基甘氨醇(Ⅲ)出发,合成了N-取代邻苯二甲酰亚胺(Ⅴ)。
First , starting from phthalic anhydride ( II ) and ( R ) - ( - ) - phenylglycinol ( III ), we prepared N-substituted phthalimide ( V ) .