氟乙酸
- 网络TFA;Fluoroacetate;fluoroacetic acid;MFA
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三氟乙酸对氨基酸催化不对称直接Aldol反应的影响
Effects of TFA on Amino Acids Catalyzed Asymmetric Direct Aldol Reaction
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区域环境中三氟乙酸富积多相传质模型研究
Multiphase Mass Transfer Model on the Accumulation of TFA in Regional Environments
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三氟乙酸溶液中尼龙6链凝聚缠结的NMR弛豫研究
Nuclear Magnetic Resonance Relaxation of Cohesional Entanglement of Nylon 6 Chains in Trifluoroacetic Acid Solution
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三氟乙酸修饰TiO2纳米微粒的制备及磨擦学性能
Preparation and Tribological Properties of TiO_2 Nanoparticles Modified by Trifluoroacetic Acid
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流动相A为1%的三氟乙酸溶液,B为乙腈-甲醇(75:25);
The mobile phase was consisted of 1 % trifluoroacetic acid solution as mobile phase A and acetonitrile - methanol ( 75:25 ) as mobile phase B with UV detection at 275 nm .
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三氟乙酸和丙三醇双掺TGS晶体生长与性能研究
Study on Growth and Properties of Doped TGS Crystal THREE-SPIN THEORY
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掺三氟乙酸TGS晶体生长及其性能研究
Study on Growth and Properties of Trifluoroacetic Acid Doped TGS Crystals
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右侧杏仁核注射β淀粉样肽(Aβ2535)制备AD大鼠模型,假手术组同样部位注射三氟乙酸;
The AD rat models were established by injecting amyloid-beta peptide ( A β _ 25-35 ) into right amygdala . The sham-operation rats were injected with trifluoroacetic acid in the same location .
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氧化反应:室温条件下氧化24h,三氟乙酸与双氧水的体积比为1∶10。
For the oxidation reaction , under the conditions of 24h and room temperature , the volume proportion of trifluoroacetic acid and H_2O_2,1 ∶ 10 .
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本文研究了水中微量三氟乙酸(TFA)的衍生化-气相色谱检测方法。
This study was focused on the determination of trace trifluoroacetic acid ( TFA ) with derivation-gas chromatography .
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流动相:A相为0.2%的三氟乙酸水溶液,B相为含0.1%的三氟乙酸的乙腈溶液,线性梯度程序为:开始10%B;
The mobile phase was ( A ) aqueous trifluoroacetic acid solution ( 0.2 % ) solution and ( B ) acetonitrile trifluoroacetic acid solution ( 0.1 % ) . The gradient elution was modified as follows : initial 10 % B ;
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探讨了三氟乙酸盐受热分解(TFAMOD)方法在多晶织构Ag基片上制备YBCO膜的工艺参数与薄膜的成分和取向、表面形貌及超导电性之间的关系。
The influences of processing parameters on phase purity and texture , surface morphology and superconducting properties of YBCO films fabricated by TFA-MOD method were discussed .
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两个Schiff碱型离子液体是一个碱分子与两个乙酸或三氟乙酸成盐,其分子式分别为:SB(CH3COO)2和SB(CF3COO)2;
The molecular formula of the two based on Schiff base cation are SB ( CH3COO ) 2 and SB ( CF3COO ) 2 ;
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然后使用反相高效液相色谱(RP-HPLC)对免疫九肽的三氟乙酸残留和有关物质进行分析,之后进行无菌检测,考察了产品质量。
And then used high performance liquid chromatography ( RP-HPLC ) to analyze trifluoroacetic acid residues and related substances , and after aseptic testing , we inspected the quality of products .
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采用1D和2DNMR技术,归属了三氟乙酸(TFA)溶液中尼龙6链上的主要1HNMR共振信号。
An unambiguous assignment of the main 1H NMR resonance of nylon 6 in trifluoroacetic acid ( TFA ) solution was carried out by using a combination of 1D and 2D NMR heteronuclear technique ( HMQC ) .
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方法采用HPLC法,C18柱,流动相为甲醇0.1%三氟乙酸水溶液(75∶25),检测波长为293nm。
METHOD HPLC method was used to carry out the determination , with C 18 Column , methanol-0.1 % trifluoroacetic acid water solution as the mobile phase ( 75 ∶ 72 ), and a wavelength of 293 nm .
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三氟乙酸是HFC-134a等氯氟烃替代品的降解产物,对植物和土壤微生物群落的生长有一定抑制作用。
Trifluoroacetic acid ( TFA ) is degradation product of some CFCs alternatives , such as HFC-134a , which has some inhibitory effects on plants and soil microbial communities .
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结果表明,采用乙腈和0.1%三氟乙酸组成的二元梯度洗脱程序,标准混合液中PCn等5种巯基化合物15min内得到很好的分离。
The results showed that by using ACN-0.1 % TFA binary gradient elution , PC_n and other thiol-containing compounds in the mixed standard solutions were rapidly separated within 15 min.
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我们对LLM-105生成过程中的三氟乙酸进行了回收,但效果不理想,三氟乙酸占了整个LLM-105生成的一半成本,对其回收有很高的经济价值。
Trifluoroacetic acid accounted for half of the cost of in the synthesis process of LLM-105 , so the recycle is with high economic value .
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乙腈-0.05%三氟乙酸溶液(70.5:29.5)为流动相;流速0.8mL·mim-1;
The mobile phase was acetonitrile - 0.05 % trifluoro - acetic acid solution ( 70.5:29.5 ) .
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此方法较水中MC测定的国家标准方法,不仅省去三氟乙酸的使用,运行时间还得以缩短,大大降低MC检测的成本。
This method saves the use of drugs trifluoroacetic acid and greatly reducing the cost of MC detection because it can shorten the running time . So the method significantly reduce the cost of MC detection when it is compared with the water method of MC determination of national standards .
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对LLM-105的工艺改进方面研究了甲氧基化、不同硝化体系、氨化条件、三氟乙酸与双氧水的体积比等因素对LLM-105总产率的影响,并优化了合成条件,确定了最佳工艺条件。
Investigated the effects of methoxylation reaction , the different nitration system , the different amination system and the volume proportion of trifluoroacetic acid and hydrogen peroxide on the total yield of LLM-105 .
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通过采用氨基与羧基的保护,DCC的合成及三氟乙酸的脱胺等方法成功合成了二肽化合物,并通过ESI-MS、1H-NMR、IR等手段对产物进行表征。
By the protection of the amido and the carboxy , combining with DCC and taking off an amine as three fluorine acetic acid , two peptides have been synthesized successfully . Then they have been characterized , assigned and analyzed by ESI-MS , 1H-NMR , IR . 3 .
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03012801为色谱柱,甲醇∶0.1%三氟乙酸水溶液(60∶40)为流动相;流速:1.0ml·min-1;
03012801 as analytic column , methanol-0.1 % trifluoroacetic Acid ( 60 ∶ 40 ) as mobile phase , the flow rate being 1.0 ml · min ~ - 1 , the detection wavelength at 273 nm .
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三氟乙酸盐-金属有机沉积技术(TFA-MOD)是制备钇钡铜氧涂层导体的有发展前景的方法之一。
The metal organic deposition ( MOD ) of YBa_2Cu_3O_ ( 7-x )( YBCO ) using metal trifluoroacetate ( TFA ) precursor is considered to be a strong candidate as a low-cost fabrication process in coated conductors .
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应用PPy-DEHS(2-(2-乙基己基)硫代丁二酸钠盐掺杂聚吡咯,溶剂为三氟乙酸)电解质装配的固体钽电解电容器具有较高的电容量和较低的损耗。
The capacitors prepared with PPy-DEHS ( PPy powder doped with di ( 2-ethylhexyl ) sulfosuccinate sodium salt ) electrolyte in trifluoroacetic acid show high capacitance and low tan δ .
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色谱条件为:ODS-AM-303色谱柱(YMC,4.6mm×250mm,5μm),柱温40℃,含0.1%三氟乙酸的乙腈-水(40∶60)为流动相,流速1mL/min。
The chromatographic conditions are as follows : ODS-AM-303 column ( YMC , 4.6mm × 250mm , 5 μ m ) with the temperature of 40 ℃, acetonitrile-water ( 40:60 ) containing 0.1 % trifluoroacetic acid as mobile phase with the flow rate of 1mL / min.
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三氟乙酸泥浆解堵固砂剂
Plug removal and sand consolidation agent of tri-fluorine acetic acid mud
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氟乙酸和氟乙酰氯的制备
A note on the preparation of FLUOROACETIC acid and fluoroacetyl chloride
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氟利昂替代品降解产物&三氟乙酸对水环境的潜在影响
Potential accumulation of Trifluoroacetates CFC-replacement degradation product in water